TY - JOUR
T1 - Synthesis and characterization of 3, 3'-Bis(tetrazol-5-yl)difurazanyl ether
AU - Li, Hui
AU - Wang, Bo Zhou
AU - Yu, Qian Qian
AU - Li, Ya Nan
AU - Shang, Yan
PY - 2012/2
Y1 - 2012/2
N2 - 3, 3'-Bis(tetrazol-5-yl)difurazanyl ether was designed and synthesized with a yield of 46.7% from 3-amino-4-cyano furazan through oxidation, ertherification and cyclization, and was characterized by 13C NMR, IR, MS and elemental analysis. In addition, the mechanism of cyclization promoted by Zn 2+ was proposed and discussed, and the reaction conditions of cyclization were optimized as follows: time is 4 h, ZnCl 2·2H 2O as catlyst, molar ratio of ZnCl 2·2H 2O to FOF-2 is 1:1.
AB - 3, 3'-Bis(tetrazol-5-yl)difurazanyl ether was designed and synthesized with a yield of 46.7% from 3-amino-4-cyano furazan through oxidation, ertherification and cyclization, and was characterized by 13C NMR, IR, MS and elemental analysis. In addition, the mechanism of cyclization promoted by Zn 2+ was proposed and discussed, and the reaction conditions of cyclization were optimized as follows: time is 4 h, ZnCl 2·2H 2O as catlyst, molar ratio of ZnCl 2·2H 2O to FOF-2 is 1:1.
KW - Difurazanyl ether
KW - Nitrogen-rich compound
KW - Organic chemistry
KW - Tetrazole
UR - http://www.scopus.com/inward/record.url?scp=84863392038&partnerID=8YFLogxK
U2 - 10.3969/j.issn.1006-9941.2012.01.005
DO - 10.3969/j.issn.1006-9941.2012.01.005
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AN - SCOPUS:84863392038
SN - 1006-9941
VL - 20
SP - 18
EP - 21
JO - Hanneng Cailiao/Chinese Journal of Energetic Materials
JF - Hanneng Cailiao/Chinese Journal of Energetic Materials
IS - 1
ER -