31P NMR methods for the direct determination of ADP in the presence of ATP

Dafna Ben-Bashat; Hadassah Shinar; Gil Navon

doi:10.1006/jmrb.1996.0038

³¹P NMR methods for the direct determination of ADP in the presence of ATP

Dafna Ben-Bashat^*, Hadassah Shinar, Gil Navon

^*Corresponding author for this work

Research output: Contribution to journal › Article › peer-review

Abstract

A new method is presented for the direct measurement of the amount of ADP in the presence of ATP by selectively eliminating the α- and γ-ATP signals. The method is compared with other methods, both experimentally and theoretically, using the product-operator formalism. An analysis of the effect of B₁ inhomogeneity on the efficiency of the methods is also given. Experimental results obtained using adiabatic pulses to compensate for such effects are shown. The accuracy of this new method is demonstrated by measuring various ADP concentrations in a series of solutions containing ADP and ATP.

Original language	English
Pages (from-to)	231-239
Number of pages	9
Journal	Journal of Magnetic Resonance - Series B
Volume	110
Issue number	3
DOIs	https://doi.org/10.1006/jmrb.1996.0038
State	Published - 1996

Access to Document

10.1006/jmrb.1996.0038

Cite this

@article{1f055f0faee149ff9f5f97aaa8e757a8,

title = "31P NMR methods for the direct determination of ADP in the presence of ATP",

abstract = "A new method is presented for the direct measurement of the amount of ADP in the presence of ATP by selectively eliminating the α- and γ-ATP signals. The method is compared with other methods, both experimentally and theoretically, using the product-operator formalism. An analysis of the effect of B1 inhomogeneity on the efficiency of the methods is also given. Experimental results obtained using adiabatic pulses to compensate for such effects are shown. The accuracy of this new method is demonstrated by measuring various ADP concentrations in a series of solutions containing ADP and ATP.",

author = "Dafna Ben-Bashat and Hadassah Shinar and Gil Navon",

year = "1996",

doi = "10.1006/jmrb.1996.0038",

language = "אנגלית",

volume = "110",

pages = "231--239",

journal = "Journal of Magnetic Resonance - Series B",

issn = "1064-1866",

publisher = "Academic Press Inc.",

number = "3",

}

TY - JOUR

T1 - 31P NMR methods for the direct determination of ADP in the presence of ATP

AU - Ben-Bashat, Dafna

AU - Shinar, Hadassah

AU - Navon, Gil

PY - 1996

Y1 - 1996

N2 - A new method is presented for the direct measurement of the amount of ADP in the presence of ATP by selectively eliminating the α- and γ-ATP signals. The method is compared with other methods, both experimentally and theoretically, using the product-operator formalism. An analysis of the effect of B1 inhomogeneity on the efficiency of the methods is also given. Experimental results obtained using adiabatic pulses to compensate for such effects are shown. The accuracy of this new method is demonstrated by measuring various ADP concentrations in a series of solutions containing ADP and ATP.

AB - A new method is presented for the direct measurement of the amount of ADP in the presence of ATP by selectively eliminating the α- and γ-ATP signals. The method is compared with other methods, both experimentally and theoretically, using the product-operator formalism. An analysis of the effect of B1 inhomogeneity on the efficiency of the methods is also given. Experimental results obtained using adiabatic pulses to compensate for such effects are shown. The accuracy of this new method is demonstrated by measuring various ADP concentrations in a series of solutions containing ADP and ATP.

UR - http://www.scopus.com/inward/record.url?scp=0030093947&partnerID=8YFLogxK

U2 - 10.1006/jmrb.1996.0038

DO - 10.1006/jmrb.1996.0038

M3 - מאמר

AN - SCOPUS:0030093947

VL - 110

SP - 231

EP - 239

JO - Journal of Magnetic Resonance - Series B

JF - Journal of Magnetic Resonance - Series B

SN - 1064-1866

IS - 3

ER -

³¹P NMR methods for the direct determination of ADP in the presence of ATP

Abstract

Access to Document

Other files and links

Fingerprint

Cite this