Solvent-free condensation of pyrrole and pentafluorobenzaldehyde: A novel synthetic pathway to corroie and oligopyrromethenes

Zeev Gross; Nitsa Galili; Liliya Simkhovich; Irena Saltsman; Mark Botoshansky; Dieter Blǎser; Roland Boese; Israel Goldberg

doi:10.1021/ol990739h

Solvent-free condensation of pyrrole and pentafluorobenzaldehyde: A novel synthetic pathway to corroie and oligopyrromethenes

Zeev Gross^*, Nitsa Galili, Liliya Simkhovich, Irena Saltsman, Mark Botoshansky, Dieter Blǎser, Roland Boese, Israel Goldberg

^*Corresponding author for this work

School of Chemistry

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Abstract

(Matrix presented) The solvent-free condensation of pyrrole and pentafluorobenzaldehyde (and to a lesser extent other electron-poor aldehydes as well) leads to a variety of products, of which three have been isolated and fully characterized. The two main products (11% each) are an open-chain pentapyrrole and corrole, a tetrapyrrolic macrocycle.

Original language	English
Pages (from-to)	599-602
Number of pages	4
Journal	Organic Letters
Volume	1
Issue number	4
DOIs	https://doi.org/10.1021/ol990739h
State	Published - 26 Aug 1999

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title = "Solvent-free condensation of pyrrole and pentafluorobenzaldehyde: A novel synthetic pathway to corroie and oligopyrromethenes",

abstract = "(Matrix presented) The solvent-free condensation of pyrrole and pentafluorobenzaldehyde (and to a lesser extent other electron-poor aldehydes as well) leads to a variety of products, of which three have been isolated and fully characterized. The two main products (11% each) are an open-chain pentapyrrole and corrole, a tetrapyrrolic macrocycle.",

author = "Zeev Gross and Nitsa Galili and Liliya Simkhovich and Irena Saltsman and Mark Botoshansky and Dieter Blǎser and Roland Boese and Israel Goldberg",

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T2 - A novel synthetic pathway to corroie and oligopyrromethenes

AU - Gross, Zeev

AU - Galili, Nitsa

AU - Simkhovich, Liliya

AU - Saltsman, Irena

AU - Botoshansky, Mark

AU - Blǎser, Dieter

AU - Boese, Roland

AU - Goldberg, Israel

PY - 1999/8/26

Y1 - 1999/8/26

N2 - (Matrix presented) The solvent-free condensation of pyrrole and pentafluorobenzaldehyde (and to a lesser extent other electron-poor aldehydes as well) leads to a variety of products, of which three have been isolated and fully characterized. The two main products (11% each) are an open-chain pentapyrrole and corrole, a tetrapyrrolic macrocycle.

AB - (Matrix presented) The solvent-free condensation of pyrrole and pentafluorobenzaldehyde (and to a lesser extent other electron-poor aldehydes as well) leads to a variety of products, of which three have been isolated and fully characterized. The two main products (11% each) are an open-chain pentapyrrole and corrole, a tetrapyrrolic macrocycle.

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Solvent-free condensation of pyrrole and pentafluorobenzaldehyde: A novel synthetic pathway to corroie and oligopyrromethenes

Abstract

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