Phosphorus heterocycle synthesis by RPX2 · ALX3 addition to [1,n]dienes-IX. The synthesis and structure of several oxaphosphabicyclic compounds

A. Rudi; I. Goldberg; Y. Kshman

doi:10.1016/S0040-4020(01)96776-6

Phosphorus heterocycle synthesis by RPX₂ · ALX₃ addition to [1,n]dienes-IX. The synthesis and structure of several oxaphosphabicyclic compounds

A. Rudi^*, I. Goldberg, Y. Kshman

^*Corresponding author for this work

School of Chemistry

Tel Aviv University

Research output: Contribution to journal › Article › peer-review

2 Scopus citations

Abstract

Several oxaphosphabicyclic compounds were synthesized by the reaction of methyl dihalophosphane under various conditions with 1,6-diketones and βγ-unsaturated ketones. The structure of one of the new compounds (11) was established by X-ray diffraction analysis. The ¹H- and ¹³C-NMR spectra of the new compounds, which, except for 11, served for their structure elucidation, are discussed.

Original language	English
Pages (from-to)	5267-5270
Number of pages	4
Journal	Tetrahedron
Volume	41
Issue number	22
DOIs	https://doi.org/10.1016/S0040-4020(01)96776-6
State	Published - 1985

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AB - Several oxaphosphabicyclic compounds were synthesized by the reaction of methyl dihalophosphane under various conditions with 1,6-diketones and βγ-unsaturated ketones. The structure of one of the new compounds (11) was established by X-ray diffraction analysis. The 1H- and 13C-NMR spectra of the new compounds, which, except for 11, served for their structure elucidation, are discussed.

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Phosphorus heterocycle synthesis by RPX₂ · ALX₃ addition to [1,n]dienes-IX. The synthesis and structure of several oxaphosphabicyclic compounds

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