TY - JOUR
T1 - Phosphorus heterocycle synthesis by RPX2. A1X3 addition to [1,n] dienes-VIII. The synthesis and structure of 3,9-dioxa-2, 4-diphosphabicyclo [3.3.1] nonanes
AU - Rudi, A.
AU - Reichman, D.
AU - Goldberg, I.
AU - Kashman, Y.
PY - 1983
Y1 - 1983
N2 - 3,9-Dioxa-2, 4-diphosphabicyclo [3.3.1] nonanes were synthesized by the reaction of methyl dihalophosphane with 1,5-diphenylpentan-1,5-dione in acetic acid. The structures of two (2 to 1) addition products (2 and 3) were established by X-ray diffraction analysis. The 1H and 13C NMR spectra of the new compounds are discussed.
AB - 3,9-Dioxa-2, 4-diphosphabicyclo [3.3.1] nonanes were synthesized by the reaction of methyl dihalophosphane with 1,5-diphenylpentan-1,5-dione in acetic acid. The structures of two (2 to 1) addition products (2 and 3) were established by X-ray diffraction analysis. The 1H and 13C NMR spectra of the new compounds are discussed.
UR - http://www.scopus.com/inward/record.url?scp=0347235745&partnerID=8YFLogxK
U2 - 10.1016/S0040-4020(01)90902-0
DO - 10.1016/S0040-4020(01)90902-0
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AN - SCOPUS:0347235745
SN - 0040-4020
VL - 39
SP - 3965
EP - 3969
JO - Tetrahedron
JF - Tetrahedron
IS - 23
ER -